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Anglo-Norwegian oil programme - intercalibration of analytical methods

Palmork, Karsten H.; Grahl-Nielsen, Otto; Wilhelmsen, Svein
Working paper
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CM_1978_E_22.pdf (1022.Kb)
URI
http://hdl.handle.net/11250/103315
Date
1978
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  • ICES CM documents authored by IMR scientists (1949-2011) [3138]
Original version
This report is not to be quoted without prior consultation with the General Secretary.  
Abstract
An attempt has been made to intercalibrate the analysis of three groups

of aromatic compounds present in a sample of Ekofisk crude oil using gas

chromatography - mass spectography. The results are not as good as was hoped.

Two possible sources of error have been identified, one instrumental and the

other related to the assumptions which had to be made regarding the responses

given by different compounds of the same group but of different molecular weights

or isomers of the same group. Proposals are made for overcoming these

difficulties. Wider participation is invited in a repeat exercise and in a

similar exercise involving the simpler u/v fluorescence method of analysis.
Publisher
ICES
Series
ICES CM Documents;1978/E:22

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